Novel ionic liquid 1,3-disulfonic acid imidazolium hydrogen sulfate {[Dsim] HSO4 } efficiently catalyzed N-boc protection of amines
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چکیده
منابع مشابه
1,3-Disulfonic acid imidazolium hydrogen sulfate {[Dsim]HSO4} as a highly efficient, recyclable and green catalyst for the preparation of α,α´-bis(arylidene)cycloalkanones
A highly efficient and simple method for the preparation of α,α´-bis(arylidene)cycloalkanones under solvent-free conditions has been developed. The crossed-aldol condensation of cycloalkanones (1 eq.) with arylaldehydes (2 eq.) in the presence of 2.5 mol% of ionic liquid 1,3-disulfonic acid imidazolium hydrogen sulfate {[Dsim]HSO4} afforded the title compounds in high yields and short reaction ...
متن کامل1,3-disulfonic acid imidazolium hydrogen sulfate {[dsim]hso4} as a highly efficient, recyclable and green catalyst for the preparation of α,α´-bis(arylidene)cycloalkanones
a highly efficient and simple method for the preparation of α,α´-bis(arylidene)cycloalkanones under solvent-free conditions has been developed. the crossed-aldol condensation of cycloalkanones (1 eq.) with arylaldehydes (2 eq.) in the presence of 2.5 mol% of ionic liquid 1,3-disulfonic acid imidazolium hydrogen sulfate {[dsim]hso4} afforded the title compounds in high yields and short reaction ...
متن کاملMelamine trisulfonic acid: A new, efficient and reusable catalyst for the protection of alcohols, phenols, aldehydes and amines
Tetrahydropyranylation of alcohols and phenols, acetylation of aldehydes and N-Boc protection of amines are efficiently catalyzed by melamine trisulfonic acid (MTSA). All reactions were performed at room temperature in good to high yields.
متن کاملMelamine trisulfonic acid: A new, efficient and reusable catalyst for the protection of alcohols, phenols, aldehydes and amines
Tetrahydropyranylation of alcohols and phenols, acetylation of aldehydes and N-Boc protection of amines are efficiently catalyzed by melamine trisulfonic acid (MTSA). All reactions were performed at room temperature in good to high yields.
متن کاملIonic liquid N-ethylpyridinium hydrogen sulfate as an efficient catalyst for designing indole scaffolds and their antimicrobial behavior
Ionic liquid N-ethylpyridinium hydrogen sulfate has been prepared, characterized and used as an efficient recyclable catalyst for the synthesis of a series of indoles and bis(indolyl)methanes. Latter have been further explored for their potential antimicrobial activity against E coli and Bacillus. The ionic liquid used was recycled in the end and its recovery was facilitated b...
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ژورنال
عنوان ژورنال: Scientia Iranica
سال: 2012
ISSN: 1026-3098
DOI: 10.1016/j.scient.2012.05.003